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An Alternative Synthetic Approach For 13-Benzoxazine Derivatives
Journal: International Journal of Scientific & Technology Research (Vol.3, No. 6)Publication Date: 2014-06-15
Authors : A. U GGabbas; I. A Mohammed; M. B. Ahmad;
Page : 46-48
Keywords : Keywords 1; 3-Benzoxazine derivative; Synthesis; Methylene Bromide; 2-hydroxybenzaldehyde; Aromatic amines; Condensation; Characterization;
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Abstract
ABSTRACT 13-benzoxazine derivatives were synthesized in high yield using three-step synthetic technique by the condensation of 2-hydroxybenzaldehyde with aromatic amines reducing the condensation products and replacing the usual formaldehyde with methylene bromide to achieve ring closure. The structures of the benzoxazines were confirmed by FTIR 1H and 13C NMR spectra and Mass spectroscopy.
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Last modified: 2015-06-28 03:57:56