Solid state synthesis of NiO nanoparticles from [(1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(II)] chloride
Journal: Iranian Chemical Communication (Vol.4, No. 3)Publication Date: 2016-07-01
Authors : Aliakbar Dehno Khalaji; Fatemeh Gharib;
Page : 265-272
Keywords : Nickel oxide; nanoparticles; Solid state; nickel(II) complex;
- Solid state synthesis of NiO nanoparticles from [(1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(II)] chloride
- A novel and efficient synthesis of bisindolyl methanes with using silica-supported 3-(triethoxysilyl) propane-1-ammonium chloride as reusable catalyst under solvent free conditions
- Cobalt oxide nanoparticles by solid-state thermal decomposition: Synthesis and characterization
- Ferromagnetic and Photoluminescence Properties of Fe doped Indium-Tin-Oxide Nanoparticles Synthesised by Solid State Reaction
- Growth and Characterization of 4- Aminopyridinium Nickel II Chloride
Abstract
In this paper, nickel oxide (NiO) nanoparticles have been prepared by solid state thermal decomposition of an acyclic nickel(II) complex (1,2-bis(2-formyl-3-methoxyphenyl)propane)nickel(II) chloride, [NiL]Cl2, in an electrical furnace at optimal temperature, 450 ºC for 3.5 h. The nickel(II) complex is obtained via solid state synthesis using nickel(II) chloride and tetradentate O4 acyclic ligand 1,2-bis(2-formyl-3-methoxyphenyl)propane. The structure and morphology of NiO nanoparticles are characterized by Fourier transform infrared spectroscopy (FT-IR), powder X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). XRD and TEM analysis show that NiO nanoparticles have pure and cubic phase with the average size of 5-10 nm.
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