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Synthesis of icosadeuterio-benzopinacol (benzopinacol-d20)

Journal: Journal of Medicinal and Chemical Sciences (Vol.3, No. 1)

Publication Date:

Authors : ; ; ; ;

Page : 35-40

Keywords : benzopinacol-d20; benzophenone-d10; dimerization; photo-reductive;

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Abstract

This work reports on synthesis of high yield (92%) of isosadeuterio-benzopinacol (benzopinacol-d20) via photo-reductive dimerization of benzophenone-d10. The latter compound was obtained using an improved method to achieve a material with high isotopic purity (> 99%). This material can be served for calibration of Mass spectrometric assays. In this study, it was also observed that benzophenone-d10 reacts faster than its natural abundance counterpart. However, elucidating the origin of this phenomenon will require additional work.

Last modified: 2019-07-27 17:42:18