Fe3O4 Bonded Pyridinium-3-carboxylic acid-N-sulfonic Acid Chloride as an Efficient Catalyst for the Synthesis of 3,4-dihydropyrimidin-2(1H)-ones
Journal: Chemical Methodologies (Vol.4, No. 5)Publication Date: 2020-09-01
Authors : Ardeshir Khazaei; Fatemeh Gohari-Ghalil; Mahsa Tavasoli; Mohammad Rezaei-Gohar; Ahmad Reza Moosavi-Zare;
Page : 543-553
Keywords : 3; 4-Dihydropyrimidin-2(1H)-one; Fe3O4 bonded pyridinium-3-carboxylic acid-N-sulfonic acid chloride; Magnetic reusable catalyst; Solvent-free;
Abstract
Fe3O4bonded pyridinium-3-carboxylic acid-N-sulfonic acid chloride, as a magnetic and reusable catalyst, was reported for the one-pot multi-component synthesis of some 3,4-dihydropyrimidin-2(1H)-ones by the reaction of urea, ethyl acetoacetateand various aldehyde under solvent-free conditions. The products were identified by FT-IR, 1H NMR and 13C NMR spectra and the catalyst was reused successfully for three times.
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