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Fe3O4 Bonded Pyridinium-3-carboxylic acid-N-sulfonic Acid Chloride as an Efficient Catalyst for the Synthesis of 3,4-dihydropyrimidin-2(1H)-ones

Journal: Chemical Methodologies (Vol.4, No. 5)

Publication Date:

Authors : ; ; ; ; ;

Page : 543-553

Keywords : 3; 4-Dihydropyrimidin-2(1H)-one; Fe3O4 bonded pyridinium-3-carboxylic acid-N-sulfonic acid chloride; Magnetic reusable catalyst; Solvent-free;

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Abstract

Fe3O4bonded pyridinium-3-carboxylic acid-N-sulfonic acid chloride, as a magnetic and reusable catalyst, was reported for the one-pot multi-component synthesis of some 3,4-dihydropyrimidin-2(1H)-ones by the reaction of urea, ethyl acetoacetateand various aldehyde under solvent-free conditions. The products were identified by FT-IR, 1H NMR and 13C NMR spectra and the catalyst was reused successfully for three times.

Last modified: 2020-07-07 21:31:48