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Rapid and green synthesis of tetrahydrobenzo[b]pyran derivatives using reusable [EMIM][OH] ionic liquid

Journal: Asian Journal of Green Chemistry (Vol.4, No. 4)

Publication Date:

Authors : ; ; ; ;

Page : 379-386

Keywords : Tetrahydrobenzo[b]pyran; Microwave irradiation; Ethyl methyl imidazolium hydroxide ionic liquid;

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Abstract

Ethyl methyl imidazolium hydroxide [EMIM][OH] ionic liquid catalyzed green protocol was developed for efficient and one-pot three-component condensation of various aromatic aldehydes, malononitrile, and dimedone under microwave irradiation for the synthesis of tetrahydrobenzo[b]pyran derivatives. The reaction proceeds in a short time period to afford moderate to excellent yield of products. The ionic liquid was recycled and reused for multiple time significantly, without a change in its catalytic efficiency. 

Last modified: 2020-09-01 01:55:59