TiCl3-silica: A recyclable solid support for efficient synthesis of substituted imidazoles
Journal: Asian Journal of Nanoscience and Materials (Vol.4, No. 1)Publication Date: 2021-01-21
Authors : Raju Subba; Hridoydip Ranjan Dasgupta; Bittu Saha; Gyan Chandra Pariyar; Abiral Tamang; Pranab Ghosh;
Page : 31-45
Keywords : 2; 4; 5-trisubstituted imidazoles Solvent free Recyclable One-pot;
Abstract
In this research study, a library of highly substituted imidazoles were efficiently synthesized from benzil/benzoin, aldehydes and ammonium acetate via multicomponent solvent free one pot protocol on TiCl3-silica solid catalyst. The general applicability of the solid support was assessed by the synthesis of wide varieties of imidazole derivatives. TiCl3-silica solid catalyst was recycled, reused and found no loss of catalytic activity up to fifth consecutive reaction runs.
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Last modified: 2021-01-22 17:04:55