The synthesis of carbethoxyhydrazine and carbethoxyhydrazone of acetophenone
Journal: Science Journal "NovaInfo" (Vol.126, No. 1)Publication Date: 2021-06-15
Authors : Zachinyaev Yaroslav Vasilevich; Zachinyaeva Anna Vladimirovna;
Page : 4-6
Keywords : CARBETHOXYHYDRAZINE; CARBETHOXYHYDRAZONE OF ACETOPHENONE; NEW CHEMICAL COMPOUNDS; SYNTHESIS; SPECTROSCOPY; ELEMENTAL MICROANALYSIS;
- The synthesis of carbethoxyhydrazine and carbethoxyhydrazone of acetophenone
- Preparation of carbethoxyhydrazone of benzalacetophenone and carbethoxyhydrazone of p-N, N-dimethylaminobenzaldehyde
- The interaction of olygomers of hexafluoropropene oxide with carbethoxyhydrazine
- Synthesis of carbethoxyhydrazone of ω-bromo-p-nitroacetophenone
- Synthesis of carbethoxyhydrazone of α-ketoglutaric acid
Abstract
This article describes the methods for the synthesis of carbethoxyhydrazine from diethyl carbonate and hydrazine hydrate and carbethoxyhydrazone of acetophenone from carbethoxyhydrazine and acetophenone when heated in methanol in the presence of catalytic amounts of glacial acetic acid.
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Last modified: 2021-06-16 18:19:43