Bio-Based Polymers Derived and Modified on Cis-1, 3,4, 6-Tetrahydrophthalimide and Its Applications
Journal: Chemical Methodologies (Vol.6, No. 9)Publication Date: 2022-09-01
Authors : Muna I. Khalaf; Asmaa Mohammed Noori Khaleel;
Page : 710-719
Keywords : Adepoyl chloride; phthalimides substituted; biobasedpolymerization;
Abstract
In the current work, N-substituted cis-1,3,4,6-tetra hydrophthalimide polymerized derivatives were prepared as bio-based materials. This research was carried out through the following three steps; Firstly, preparing N-alkyl cis-1,3,4,6-tetra hydrophthalamic acid by reacting of cis-1,3,4,6-tetra hydrophthalimide salt with (benzyl chloride, PVC, adipoyl chloride, co-poly vinyl acetate chloride and poly acyloyl chloride) respectively producing, N-alkyl tetra hydro phthalimide. Furthermore, the next step includes preparing N-creatinyl tetrahydro phthal imide, and followed by the polymerization step of the prepared unsaturated compounds throughutilizing (BPO) as initiator alongside the heating. Several techniques were used to characterize the prepared compounds such as recording the melting points and softening point as well as infrared spectroscopy (FTIR). However, some of the prepared compounds were characterized by using proton nuclear magnetic resonance 1HNMRand studied thermally via differential scanning calorimetric technique DSC.
Other Latest Articles
- Assessment of MoTiO3/GO Integrated Photocatalyst for Converting CO2 to Methanol
- Improving Rheological and Sensory Properties of Flour and Laboratory Cake Using Different Concentrations of Guar Gum
- Design, Synthesis, Docking and Biological Study of Pyrazole-3,5-diamine Derivatives with Potent Antitubercular Activity
- Adsorption and Photocatalytic Degradation of Crystal Violet Dye under Sunlight Irradiation Using Natural and Modified Clays by Zinc Oxide
- Synthesis and Characterization of New Demulsifier from Natural Polymer
Last modified: 2022-07-10 18:03:13