Construction of a Novel Magnetic Nanomaterial, and its Utility as an Effectual Catalyst for the Fabrication of 1, 8-Dioxo-Octahydroxanthenes
Journal: Chemical Methodologies (Vol.8, No. 1)Publication Date: 2024-01-01
Authors : Abdolkarim Zare; Fatemeh Mostaghar;
Page : 23-36
Keywords : Magnetic nanomaterial; STCDFS; 1; 8-Dioxo-octahydroxanthene; Solvent-free;
Abstract
At first, construction and characterization of a novel magnetic nanomaterial titled N1-(Si-pr)-(N1,N1,N4,N4-tetramethylbenzene-1,4-diaminium) chloride dihydrogen phosphate grafted on Fe3O4@SiO2 (STCDFS) have been described. The characterization has been accomplished by EDX, elemental mapping, FE-SEM, FT-IR, XRD, and VSM analyses. In continue, effectual and quick fabrication of 1,8-dioxo-octahydroxanthenes form aryl aldehydes and dimedone using STCDFS in solvent-free conditions has been reported. The xanthenes were acquired in 92-98% in 5-10 min. Moreover, the catalyst was reusable for one time without remarkable decrement in its performance.
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Last modified: 2024-01-01 16:14:51