SYNTHESIS STRUCTURAL AND MAGNETIC PROPERTIES OF TITANIUM DOPED MAGNESIUM ZINC FERRITE
Journal: International Education and Research Journal (Vol.10, No. 8)Publication Date: 2024-08-15
Authors : Sruthi P.;
Page : 70-72
Keywords : Titanium Doped Magnesium Zinc Ferrite; X-Ray Diffraction(XRD); Fourier Transformer Infrared Spectroscopy (FTIR); Nano Particles (NPS); Curie Temperature;
Abstract
Magnetic ceramics or ferrites are very well established group of magnetic materials which exhibits ferrimagnetism. It possess high electrical resistivity, low eddy current and dielectric loss which makes it superior than the other ordinary magnetic oxides that contain the ferric oxide (Fe₂O₃) as their basic magnetic compounds. The ceramic magnets are widely used in high frequency transformer application. [(Mg, Mn, F12o4)] spinels are used in square-loop application. Ceramic materials found application in nuclear physics. In nuclear reactors ceramics are used as core components. The studies include the preparation and analysis of Titanium doped Magnesium zinc ferrite. Here, Titanium doped magnesium zinc ferrite nanoparticles (NPS) were synthesized using solid state reaction method. Titanium doping can enhance the magnetic properties of magnesium zinc ferrite in several ways these can contribute to improved magnetic properties , such as increased magnetic moment, saturation magnetization, and magnetic ordering , making titanium – doped magnesium zinc ferrite a promising material for various applications including magnetic storage, sensors, and spintronics. According to the stoichiometric equation [Mg0.9Zn 0.1TixFe2-xO4] at different values of x, (x=0.1, 0.3) are synthesised. Calcination and sintering of the samples is made by high temperature PID controlled muffle furnace which can go up to 1000°C. The structural and magnetic properties are examined using XRD, FTIR and Curie temperature analysis. From the XRD analysis it revels the phase structure and lattice parameters of the samples. XRD analysis gives maximum intensity of (h k l) values as (3 1 1) in both cases. It also reveals that no secondary phases are produced during growth. That means the specimens FCC stacking. FTIR analysis of the samples done using Fourier transformer infrared spectroscopy. From this analysis it revels the detailed atomic structure and bonding of the samples. The bands obtained reveal spinal ferrite structure. Curie temperature of the specimens is determined by Curie temperature apparatus for the study of magnetic properties of the specimens.
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