Effect of Microstructure Evolution and Corrosion Behavior on Phase Transformation of Nanocrystalline SUS304 Prepared by Dry Ice Shot Peening

Microstructure and corrosion behavior of nanocrystalline SUS304 by dry ice shot peening has been investigated in detail in term of phase transformation. SUS304 as metastable austenitic stainless has excellent corrosion resistance and induced martensite by shot peening process. However, the SUS304 has quite low strength which is difficult to wear as metallic component. The dry ice shot peening process was carried out on SUS304 surface for one and three hours. The microstructure was observed by transmission electron microscope (TEM) and scanning electron microscope (SEM) equipped with electron back-scattered diffraction (EBSD). The phase transformation was analyzed by X-ray diffraction (XRD). The corrosion testing was carried out in 3.5% NaCl solution. The result indicated that the grain size of SUS304 surface was finer by deformation due to dry ice shot peened process. The hardness was improved properly by the increasing the shot peened time, and the corrosion resistance was increased. The XRD results showed that three hours shot peening process induced martensite phase of SUS304 by 15 m thickness. It can be summarized that the dry ice shot peening can be induced phase transformation due to high deformation on the SUS304 surface