Temperature Based Investigation on Structure and Optical Properties of Bi2S3 Nanoflowers by Solvothermal Approach
Journal: Mechanics, Materials Science & Engineering Journal (Vol.9, No. 1)Publication Date: 2017-05-04
Authors : J. Arumugam; A. Dhayal Raj; A. Albert Irudayaraj; T. Pazhanivel;
Page : 181-187
Keywords : Bi2S3 nanostructures; XRD; SEM; UV-Vis; FTIR;
Abstract
A solvothermal process has been employed to synthesis Bi2S3 nanostructures which has a wide spread applications in photodiode, hydrogen storage, high energy batteries, as well as luminescence and catalytic fields. Bismuth nitrate, thiourea and PolyVinyPyrrolidene (PVP), used as the starting materials are dissolved in ethylene glycol for different reaction times. It was found that the temperature plays a key role in determining the shape of the products. The crystalline phase and structure of the Bi2S3 nanostructures were investigated by power X-ray diffraction (XRD). The surface morphology has been analyzed by Scanning electron microscopy (SEM), the optical properties of the Bi2S3 nanoparticles were analyzed using UV-Vis spectroscopy. The functional groups present in the Bi2S3 nanoparticles were characterized by FT-IR spectroscopy. The novel Bi2S3 nanoparticles will be exploited for its application as photocatalyst.
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Last modified: 2017-09-05 19:06:07