SYNTHESIS AND STUDY OF BIMETALLIC CATALYTIC SYSTEMS FORMED IN SITU BY ALUMINUM, 1, 2-DICHLOROETHANE AND Fe (III), Ni (II), Mn (II) CHLORIDES
Journal: Journal of Advances in Chemistry (Vol.3, No. 1)Publication Date: 2013-08-10
Authors : K.M. Gasimova; H.J. Ibragimov; Z.M. Ibragimova; I.V. Kolchikova; Mai M. Khalaf; A.E. Alieva;
Page : 120-132
Keywords : CTC; CTC/FeCl3; CTC/NiCl2; CTC/MnCl2; XRFM; TG/DSC; XRD;
Abstract
Novel bimetallic catalytic systems based on the catalytic complex (CTC) are synthesized from the reaction of Al metal and 1, 2-dichloroethane in the mode of in situ and modified with the metal chlorides of Mn (II), Fe (III), and Ni (II) in paraffin medium. The structures of synthesized catalytic samples were confirmed by bulk and surface characterization with FTIR, X-ray diffraction (XRD), thermal analyses (TG/DTG/DTA), dynamic light scattering spectroscopy (DLS) for determination the particle size and X-ray fluorescence microscopy (XRFM).
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