PHOTOELECTROCHEMICAL SYNTHESIS OF OLIGOTETRAMETHYLENDIAMIDODISULPHOIMIDE OF DISACCHARIN OF CARBOXYLIC ACID
Journal: Azerbaijan Chemical Journal (Vol.0, No. 1)Publication Date: 2018-03-28
Authors : E.M.Guliyev T.A.Aslanov E.T.Aslanova M.N.Rashidova;
Page : 111-114
Keywords : the photoelectrochemical oxidative polycondensation; tetramethylen-diamidodisulphoimide of disaccharin of carboxylic acid; visible light; inhibitor; oligomer; gravimetric method;
Abstract
The reaction of photoelectrochemical oxidative polycondensation of tetramethylendiamido-disulphoimide of disaccharin of carboxylic acid has been investigated by method of electrolysis in an aqueous solution of suphuric acid under irradiation with visible light. It has been established that increasing the amount of electricity passed through the medium up to 16 A•h yield of synthesized oligomers of tetramethylendiamidodisulphoimide of disaccharin of carboxylic acid is 80–82%. An effect of the obtained oligomers as corrosion inhibitors in acidic medium has been studied
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